Synthesis Videos

Preparation of TiCl3(THF)3

This is the preparation of TiCl3(THF)3TiCl3

AlCl3 + PhMe + THF → TiCl3(THF)3 + AlCl3 + (THF)n

Soxhlet extraction

The use of the soxhlet apparatus for the solvation and extraction of CrCl3(THF)3 is presented here.