Preparation of TiCl3(THF)3This is the preparation of TiCl3(THF)3TiCl3AlCl3 + PhMe + THF → TiCl3(THF)3 + AlCl3 + (THF)n Soxhlet extractionThe use of the soxhlet apparatus for the solvation and extraction of CrCl3(THF)3 is presented here.